CHE 310 L
Organic Chemistry I Laboratory
Spring 2012

Experiments

#	Experiment	Download
	Introduction
1.	Melting point
2.	Unknown recrystallization and Identification
3.	Thin Layer Chromatography
4.	Acid-Base Extraction
5.	Column Chromatography
6.	Molecular Modeling Using ChemSketch Chemical Drawing Software
7.	Introduction to NMR Spectroscopy NMR spectra
8.	Aldehydes and Ketones
9.	Carbocation rearrangement
10.	Separation and Spectroscopy
11. & 12.	pH Controlled Oxidation of an Aromatic Ketone #1 & #2	NMR SM NMR base rxn NMR acid rxn

Additional Material

The information below can be downloaded in pdf format by clicking on the appropriate colored ball. Materials for all faculty

Item	Download
Accuracy, Precision and Significant Figures
Running the NMR spectrometer
SymyxDraw Software Using SymyxDraw Chemical Drawing Software
Download ChemSketch

You will need the following for the first day:

1. Safety glasses
These can be purched in lab on the first day from
The Student Affiliates of The American Chemical Society.
New Visorgogs ar $8; used Visorgogs $6 (while supplies last).
CASH ONLY

2. A laboratory notebook (available from the bookstore)

3. The text book The techniques you will need are described in the required text: Techniques in Organic Chemistry, 3rd Ed Authors: Mohrig, Hammond and Schatz W.H. Freeman and Co., NY; 2010 This book is available in the bookstore.

4. You will need to have read Introduction
The pdf file can be downloaded below.

5. Read and be prepared for the Melting point experiment
The word file can be downloaded below.

 

updated January 23, 2012 9:18 AM